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Drug safety is related to the health of the public. We hope that taking medicine can relieve pain and prolong life, but now taking medicine seems to be taking poison! Recently, GlaxoSmithKline's Amoxicillin Clavulanate Potassium Dry Suspension (domestic trade name is Leptin) was found to have been exposed to plasticizers such as diisodecyl phthalate (DIDP). The State Food and Drug Administration ordered a recall, and the sale and use of the product were also prohibited. This news once again pushed the plasticizer to the cusp, and it also made consumers confused about the choice and use of drugs.
From the discovery of plasticizers in various foods in Taiwan to the emergence of plasticizers in medicines, this chemical substance that is rarely known to ordinary people is approaching step by step in a frightening image. Dima Technology continues to develop and develop a variety of commonly used drugs in daily life (tablets-pyrithione hydrochloride tablets; injection-hydrocortisone injection; granules-Radix isatidis; syrup-Tai Chi cough syrup; suspension- Nimesulide Dry Suspension) phthalate ester detection method, I hope this method can do a good job for the safety of commonly used drugs in daily life, so that people can take rest assured medicine. This method uses organic solvents to extract the phthalate esters. After purification by ProElut PSA glass solid phase extraction cartridge, it is analyzed by HPLC and GC-MS.
Detailed detection method link: http: //SH100707/down_172278.htm
Relevant product information in the application method:
Item No. Name Brand Specification 63206G ProElut PSA Glass SPE Column Dikma ProElut 1000mg / 6ml, 30 / pkgFor more specifications and packings, please call 65584 anhydrous sodium sulfate Dikma ProElut 500g 8221 capillary gas chromatography column DM-5MS Dikma 30mm * 0.25mm * 0.25um
99603 Diamonsil C18 (2) Dikma 250 × 4.6mm, 5μm 244358 12 tubes to prevent cross contamination
Vacuum SPE extraction device imported 12-position 5323 sample vial (brown / thread) Dikma 2 mL, 100 / pk 5325 vial cap / with pad (assembled) Dikma 100 / pk 37177 syringe filter Nylon Dikma 13mm, 0.22μm 100 / pk 50123 methyl tert-butyl ether HPLC grade DikmaPure 4L 50115 n-hexane HPLC grade DikmaPure 4L 50106 acetone HPLC grade DikmaPure 4L 50101 acetonitrile HPLC grade DikmaPure 4L
About ProElut glass SPE column
The ProElut glass SPE column is dedicated to high-purity extraction. The inert glass tube completely eliminates contamination from plasticizers, including phthalates. As a standard series of ProElut series cartridges, glass extraction cartridges use high-quality ProElut adsorbents and special purification treatment sieve plates, which ensure more stability and repeatability.
Phthalates Standard
Phthalate mixed standard
1,000ug / mL mixed standard of 12-PT8061-1M phthalate in isooctane (16 components), including 1-10,12,13,15,16 components in GB / T 21911-2008 Chemservice 5ml,
1,000ug / mL mixed standard of 12-PT8061-1RPM phthalate in isooctane (16 components), including 1-10,12,13,15,16 components in GB / T 21911-2008 Chemservice 5x1mL,
1,000ug / mL in isooctane GB / T 21911-2008 phthalate 16 component single label
/ 46595 1. Dimethyl phthalate (DMP),
CAS: 131-11-3 Chemservice
/ xStandard 1g
/ 500mg 12-F70
/ 46594 2. Diethyl phthalate (DEP),
CAS: 84-66-2 Chemservice
/ xStandard 1g
/ 500mg 12-F2264
/ 46588 3. Diisobutyl phthalate (DIBP),
CAS: 84-69-5 Chemservice
/ xStandard 5g
/ 500mg 12-F68
/ 46597 4. Dibutyl phthalate (DBP),
CAS: 84-74-2 Chemservice
/ xStandard 1g
/ 500mg 12-F2268
/ 46589 5. Di (2-methoxyethyl) phthalate (DMEP),
CAS: 117-82-8 Chemservice
/ xStandard 500mg
/ 500mg 12-F2309
/ 46600 6. Di (4-methyl-2-pentyl) phthalate (BMPP),
CAS: 146-50-9 Chemservice
/ xStandard 5g
/ 500mg 12-F2312
/ 46601 7. Di (2-ethoxy) ethyl phthalate (DEEP),
CAS: 605-54-9 Chemservice
/ xStandard 500mg
/ 500mg 12-F2263
/ 46593 8. Dipentyl phthalate (DPP),
CAS: 131-18-0 Chemservice
/ xStandard 500mg
/ 500mg 12-F2314
/ 46596 9. Dihexyl phthalate (DHXP),
CAS: 84-75-3 Chemservice
/ xStandard 5g
/ 500mg 12-F67
/ 46598 10. Butyl benzyl phthalate (BBP),
CAS: 85-68-7 Chemservice
/ xStandard 1g
/ 500mg 12-F2315
/ 46590 11. Di (2-butoxy) ethyl phthalate (DBEP),
CAS: 117-83-9 Chemservice
/ xStandard 1g
/ 500mg 12-F2262
/ 46602 12. Dicyclohexyl phthalate (DCHP),
CAS: 84-61-7 Chemservice
/ xStandard 5g
/ 500mg 12-F66
/ 46592 13. Di (2-ethylhexyl) phthalate (DEHP)
CAS: 117-81-7 Chemservice
/ xStandard 1g
/ 500mg 12-F1091
/ 46591 14. Diphenyl phthalate,
CAS: 84-62-8 Chemservice
/ xStandard 5g
/ 500mg 12-F69
/ 46603 15. n-dioctyl phthalate (DNOP),
CAS: 117-84-0 Chemservice
/ xStandard 1g
/ 500mg 12-F2317
/ 46599 16. Dinonyl phthalate (DNP),
CAS: 84-76-4 Chemservice
/ xStandard 5g
/ 500mg
For more single phthalate standard, please call us
Download: 17 kinds of phthalates in various medicines and related products.pdf
About Dima
Dima Technology is a well-known chromatographic consumable manufacturer dedicated to R & D and manufacturing of scientific and efficient chemical analysis products, providing comprehensive services and comprehensive solutions. It has always been in many technical fields such as chromatographic packing research and development, chromatographic column manufacturing and related separation products Maintain the world's advanced level. Core technology products include: liquid chromatography columns, gas chromatography columns, solid phase extraction columns, chromatography solvents and chemical standards.
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